Martin Luther University Halle-Wittenberg

Further settings

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Equipment and devices


Synthesis

Autoclave
Berghof
Hydrothermal syntheses
up to 250 °C

Spin Coating Unit
Laurell WS-650MZ-23NPP/Lite

Spray Dryer
Büchi B-191

Microwave Unit
Muegge
2000 W, 850 W, 300 W

Mixing and Milling

Planetary Ball Mill
Retsch PM 400

Planetary Mill
Fritsch Pulverisette

Single Crystal Growth

Optically Heated Floating Zone Melting Furnace (Four mirror furnace)
CSC FZ-T-10000-H-HR-I-VPO-PC
Tmax > 2000 °C
10-5 mbar < p < 10 bar

Crystal Growing Unit
using Czochralski Process
Malvern MSR2
Tmax > 2000 °C

Cutting, Grinding, and Polishing

Grinding and Polishing Machine
Struers LaboPol-5

Precision Cutt-Off Machine
Struers Minitom

X-ray Diffractometry

Bragg-Brentano
X-ray Powder Diffractometer
Bruker D8 Advanced
(Cu-K radiation)

Imaging Plate
Single Crystal Diffractometer
STOE-IPDS2T
(Mo-K radiation)

Four-Cycle Single Crystal Diffractometer
STOE-STADI4
(Ag-K radiation)

Spectroscopy

UV-Vis Transmission Spectrometer
VWR UV-3100 PC

UV-Vis-NIR Reflection Spectrometer
Perkin Elmer Lambda 19

FT-IR
Infrared Spectrometer
Bruker Alpha
Transmission and reflection (ATR)

Determination of Physical Properties

Physical Properties Measurement System
Quantum Design PPMS9
2K < T < 400 K, -90 kOe < H < +90 kOe

  • Magnetism
  • Electrical conductivity
  • Specific heat
  • Thermoelectric properties
  • Hall effect

Impedance analyser
HP 4192A
1 Hz to 13 MHz with thermostate
Julabo F25, -20°C to +250°C

Gas Physisorption

Gas Physisorption Unit
Quantachrome Nova 1000

Thermal Analysis

Thermo-Analysis System
Netzsch STA 409
Simultaneous TG and DSC/DTA up to1400 °C

Thermo-Analysis System
Netzsch Jupiter
Simultaneous TAG and DSC/DTA with coupled Mass Spectrometry (not shown) up to 1400 °C

Dilamometer
Setaram TMA92
Thermal expansion/sintering behaviour up to 1500 °C

Dilamometer
Netzsch TMA 402
Thermal expansion/Sintering behaviour up to 1200 °C

Thermobalance
TA Instruments TGA 2950
Thermogravimetry up to 1000 °C

Laboratory Furnaces

Various box- and tube-furnaces with maximum working temperatures between 1100°C and 1750°C.

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