Equipment and devices
Synthesis
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Autoclave
Berghof
Hydrothermal syntheses
up to 250 °C
|
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Spin Coating Unit
Laurell WS-650MZ-23NPP/Lite
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Spray Dryer
Büchi B-191
|
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Microwave Unit
Muegge
2000 W, 850 W, 300 W
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Mixing and Milling
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Planetary Ball Mill
Retsch PM 400
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Planetary Mill
Fritsch Pulverisette
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Single Crystal Growth
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Optically Heated Floating Zone Melting Furnace (Four mirror furnace)
CSC FZ-T-10000-H-HR-I-VPO-PC
Tmax > 2000 °C
10-5 mbar < p < 10 bar
|
|
Crystal Growing Unit
using Czochralski Process
Malvern MSR2
Tmax > 2000 °C
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Cutting, Grinding, and Polishing
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Grinding and Polishing Machine
Struers LaboPol-5
|
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Precision Cutt-Off Machine
Struers Minitom
|
X-ray Diffractometry
|
Bragg-Brentano
X-ray Powder Diffractometer
Bruker D8 Advanced
(Cu-K radiation)
|
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Imaging Plate
Single Crystal Diffractometer
STOE-IPDS2T
(Mo-K radiation)
|
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Four-Cycle Single Crystal Diffractometer
STOE-STADI4
(Ag-K radiation)
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Spectroscopy
|
UV-Vis Transmission Spectrometer
VWR UV-3100 PC
|
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UV-Vis-NIR Reflection Spectrometer
Perkin Elmer Lambda 19
|
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FT-IR
Infrared Spectrometer
Bruker Alpha
Transmission and reflection (ATR)
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Determination of Physical Properties
|
Physical Properties Measurement System
Quantum Design PPMS9
2K < T < 400 K, -90 kOe < H < +90 kOe
- Magnetism
- Electrical conductivity
- Specific heat
- Thermoelectric properties
- Hall effect
|
|
Impedance analyser
HP 4192A
1 Hz to 13 MHz with thermostate
Julabo F25, -20°C to +250°C
|
Gas Physisorption
|
Gas Physisorption Unit
Quantachrome Nova 1000
|
Thermal Analysis
|
Thermo-Analysis System
Netzsch STA 449F5
Simultaneous TG and DSC/DTA up to 1500 °C
|
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Thermo-Analysis System
Netzsch Jupiter
Simultaneous TAG and DSC/DTA with coupled Mass Spectrometry (not shown) up to 1400 °C
|
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Dilamometer
Netzsch TMA 402 F3
Thermal expansion/sintering behaviour up to 1500 °C
|
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Dilamometer
Netzsch TMA 402
Thermal expansion/sintering behaviour up to 1200 °C
|
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Thermobalance
TA Instruments TGA 2950
Thermogravimetry up to 1000 °C
|
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Deep-temperature DSC (Dynamic Differential Calorimeter)
Setaram 131 evo
Temperature range from -150 °C to 500 °C
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Chemical Analysis
|
Flame Atomic Absorption
Spectrometer (AAS) Agilent 280FS
with autosampler and
automatic dilution device
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Laboratory Furnaces (Selection)
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Various box- and tube-furnaces with maximum working temperatures between 1100°C and 1750°C.
|
Scanning Electron Microscopy
|
Phenom ProX Scanning electron microscope
50000x magnification, acceleration voltage range 5 - 15 kV, BSE detector with EDX
|
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